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000824326 1001_ $$0P:(DE-HGF)0$$aBauer, A.$$b0$$eCorresponding author
000824326 245__ $$aUltra-high vacuum compatible induction-heated rod casting furnace
000824326 260__ $$a[S.l.]$$bAmerican Institute of Physics$$c2016
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000824326 520__ $$aWe report the design of a radio-frequency induction-heated rod casting furnace that permits the preparation of polycrystalline ingots of intermetallic compounds under ultra-high vacuum compatible conditions. The central part of the system is a bespoke water-cooled Hukin crucible supporting a casting mold. Depending on the choice of the mold, typical rods have a diameter between 6 mm and 10 mm and a length up to 90 mm, suitable for single-crystal growth by means of float-zoning. The setup is all-metal sealed and may be baked out. We find that the resulting ultra-high vacuum represents an important precondition for processing compounds with high vapor pressures under a high-purity argon atmosphere up to 3 bars. Using the rod casting furnace, we succeeded to prepare large high-quality single crystals of two half-Heusler compounds, namely, the itinerant antiferromagnet CuMnSb and the half-metallic ferromagnet NiMnSb.
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000824326 65017 $$0V:(DE-MLZ)GC-2002-2016$$2V:(DE-HGF)$$aInstrument and Method Development$$x0
000824326 693__ $$0EXP:(DE-MLZ)HEIDI-20140101$$1EXP:(DE-MLZ)FRMII-20140101$$5EXP:(DE-MLZ)HEIDI-20140101$$6EXP:(DE-MLZ)SR9b-20140101$$aForschungs-Neutronenquelle Heinz Maier-Leibnitz $$eHEiDi: Single crystal diffractometer on hot source$$fSR9b$$x0
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000824326 7001_ $$0P:(DE-HGF)0$$aNeubauer, A.$$b1
000824326 7001_ $$0P:(DE-HGF)0$$aMünzer, W.$$b2
000824326 7001_ $$0P:(DE-HGF)0$$aRegnat, A.$$b3
000824326 7001_ $$00000-0002-3317-538X$$aBenka, G.$$b4
000824326 7001_ $$0P:(DE-Juel1)164297$$aMeven, M.$$b5$$ufzj
000824326 7001_ $$0P:(DE-HGF)0$$aPedersen, B.$$b6
000824326 7001_ $$0P:(DE-HGF)0$$aPfleiderer, C.$$b7
000824326 773__ $$0PERI:(DE-600)1472905-2$$a10.1063/1.4954926$$gVol. 87, no. 6, p. 063909 -$$n6$$p063909 -$$tReview of scientific instruments$$v87$$x1089-7623$$y2016
000824326 8564_ $$uhttps://www.ncbi.nlm.nih.gov/pubmed/27370472
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