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| 001 | 824326 | ||
| 005 | 20210129225018.0 | ||
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| 100 | 1 | _ | |a Bauer, A. |0 P:(DE-HGF)0 |b 0 |e Corresponding author |
| 245 | _ | _ | |a Ultra-high vacuum compatible induction-heated rod casting furnace |
| 260 | _ | _ | |a [S.l.] |c 2016 |b American Institute of Physics |
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| 520 | _ | _ | |a We report the design of a radio-frequency induction-heated rod casting furnace that permits the preparation of polycrystalline ingots of intermetallic compounds under ultra-high vacuum compatible conditions. The central part of the system is a bespoke water-cooled Hukin crucible supporting a casting mold. Depending on the choice of the mold, typical rods have a diameter between 6 mm and 10 mm and a length up to 90 mm, suitable for single-crystal growth by means of float-zoning. The setup is all-metal sealed and may be baked out. We find that the resulting ultra-high vacuum represents an important precondition for processing compounds with high vapor pressures under a high-purity argon atmosphere up to 3 bars. Using the rod casting furnace, we succeeded to prepare large high-quality single crystals of two half-Heusler compounds, namely, the itinerant antiferromagnet CuMnSb and the half-metallic ferromagnet NiMnSb. |
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| 693 | _ | _ | |a Forschungs-Neutronenquelle Heinz Maier-Leibnitz |e HEiDi: Single crystal diffractometer on hot source |f SR9b |1 EXP:(DE-MLZ)FRMII-20140101 |0 EXP:(DE-MLZ)HEIDI-20140101 |5 EXP:(DE-MLZ)HEIDI-20140101 |6 EXP:(DE-MLZ)SR9b-20140101 |x 0 |
| 693 | _ | _ | |a Forschungs-Neutronenquelle Heinz Maier-Leibnitz |e RESI: Thermal neutron single crystal diffractometer |f SR8b |1 EXP:(DE-MLZ)FRMII-20140101 |0 EXP:(DE-MLZ)RESI-20140101 |5 EXP:(DE-MLZ)RESI-20140101 |6 EXP:(DE-MLZ)SR8b-20140101 |x 1 |
| 700 | 1 | _ | |a Neubauer, A. |0 P:(DE-HGF)0 |b 1 |
| 700 | 1 | _ | |a Münzer, W. |0 P:(DE-HGF)0 |b 2 |
| 700 | 1 | _ | |a Regnat, A. |0 P:(DE-HGF)0 |b 3 |
| 700 | 1 | _ | |a Benka, G. |0 0000-0002-3317-538X |b 4 |
| 700 | 1 | _ | |a Meven, M. |0 P:(DE-Juel1)164297 |b 5 |u fzj |
| 700 | 1 | _ | |a Pedersen, B. |0 P:(DE-HGF)0 |b 6 |
| 700 | 1 | _ | |a Pfleiderer, C. |0 P:(DE-HGF)0 |b 7 |
| 773 | _ | _ | |a 10.1063/1.4954926 |g Vol. 87, no. 6, p. 063909 - |0 PERI:(DE-600)1472905-2 |n 6 |p 063909 - |t Review of scientific instruments |v 87 |y 2016 |x 1089-7623 |
| 856 | 4 | _ | |u https://www.ncbi.nlm.nih.gov/pubmed/27370472 |
| 856 | 4 | _ | |u https://juser.fz-juelich.de/record/824326/files/1.4954926.pdf |y Published on 2016-06-30. Available in OpenAccess from 2017-06-30. |
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