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000835088 0247_ $$2doi$$a10.1016/j.jnucmat.2017.06.034
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000835088 0247_ $$2ISSN$$a1873-4820
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000835088 041__ $$aEnglish
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000835088 1001_ $$00000-0003-0629-3484$$aArinicheva, Yulia$$b0$$eCorresponding author
000835088 245__ $$aStructural investigations of (La,Pu)PO$_{4}$ monazite solid solutions: XRD and XAFS study
000835088 260__ $$aAmsterdam [u.a.]$$bElsevier Science$$c2017
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000835088 520__ $$aA solid state method was used to synthesize La1-xPuxPO4 (x = 0.01, 0.05, 0.10, 0.15, (0.5)) solid solutions with monazite structure. XRD measurements of the compounds with x = 0.50 revealed the formation of two phases: (La,Pu)PO4-monazite and a cubic phase (PuO2). Pure-phase La1-xPuxPO4-monazite solid solutions were obtained for materials with x = 0.00–0.15 and confirmed by a linear dependence of the lattice parameters on composition according to Vegard's law. X-ray absorption spectroscopy (XAS) analysis at the Pu-LIII and La-LIII edges confirmed the +III valence state of plutonium in the monazite solid solutions. The local environment of Pu is PuPO4-like along the solid solution series, except for the longest fitted cation-cation distance, which may be an indication of cluster formation consisting of a few Pu-atoms in the La-Pu-monazite lattice.
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000835088 7001_ $$00000-0003-2759-6492$$aPopa, Karin$$b1
000835088 7001_ $$00000-0002-6608-5428$$aScheinost, Andreas C.$$b2
000835088 7001_ $$0P:(DE-HGF)0$$aRossberg, André$$b3
000835088 7001_ $$0P:(DE-HGF)0$$aDieste-Blanco, Oliver$$b4
000835088 7001_ $$0P:(DE-HGF)0$$aRaison, Philippe$$b5
000835088 7001_ $$0P:(DE-HGF)0$$aCambriani, Andrea$$b6
000835088 7001_ $$0P:(DE-HGF)0$$aSomers, Joseph$$b7
000835088 7001_ $$0P:(DE-Juel1)130324$$aBosbach, Dirk$$b8
000835088 7001_ $$0P:(DE-Juel1)130389$$aNeumeier, Stefan$$b9$$eCorresponding author
000835088 773__ $$0PERI:(DE-600)2001279-2$$a10.1016/j.jnucmat.2017.06.034$$gVol. 493, p. 404 - 411$$p404 - 411$$tJournal of nuclear materials$$v493$$x0022-3115$$y2017
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