Hauptseite > Publikationsdatenbank > Structural investigations of (La,Pu)PO$_{4}$ monazite solid solutions: XRD and XAFS study > print

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024 7 _ |a 10.1016/j.jnucmat.2017.06.034
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024 7 _ |a 1873-4820
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100 1 _ |a Arinicheva, Yulia
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245 _ _ |a Structural investigations of (La,Pu)PO$_{4}$ monazite solid solutions: XRD and XAFS study
260 _ _ |a Amsterdam [u.a.]
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520 _ _ |a A solid state method was used to synthesize La1-xPuxPO4 (x = 0.01, 0.05, 0.10, 0.15, (0.5)) solid solutions with monazite structure. XRD measurements of the compounds with x = 0.50 revealed the formation of two phases: (La,Pu)PO4-monazite and a cubic phase (PuO2). Pure-phase La1-xPuxPO4-monazite solid solutions were obtained for materials with x = 0.00–0.15 and confirmed by a linear dependence of the lattice parameters on composition according to Vegard's law. X-ray absorption spectroscopy (XAS) analysis at the Pu-LIII and La-LIII edges confirmed the +III valence state of plutonium in the monazite solid solutions. The local environment of Pu is PuPO4-like along the solid solution series, except for the longest fitted cation-cation distance, which may be an indication of cluster formation consisting of a few Pu-atoms in the La-Pu-monazite lattice.
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700 1 _ |a Popa, Karin
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700 1 _ |a Scheinost, Andreas C.
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700 1 _ |a Rossberg, André
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700 1 _ |a Dieste-Blanco, Oliver
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700 1 _ |a Neumeier, Stefan
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773 _ _ |a 10.1016/j.jnucmat.2017.06.034
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