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@ARTICLE{Arinicheva:839910,
author = {Arinicheva, Y. and Clavier, N. and Neumeier, S. and Podor,
R. and Bukaemskiy, A. and Klinkenberg, M. and Roth, G. and
Dacheux, N. and Bosbach, D.},
title = {{E}ffect of powder morphology on sintering kinetics,
microstructure and mechanical properties of monazite
ceramics},
journal = {Journal of the European Ceramic Society},
volume = {38},
number = {1},
issn = {0955-2219},
address = {Amsterdam [u.a.]},
publisher = {Elsevier Science},
reportid = {FZJ-2017-07488},
pages = {227 - 234},
year = {2018},
abstract = {This work focuses on the effect of precursor morphology on
the microstructural evolution of monazite-type
lanthanum-europium phosphate ceramics during sintering,
including grain growth rate, as well as correlations between
microstructure, texture effects and their mechanical
properties. Sintering kinetics of La0.5Eu0.5PO4 powders with
two different grain morphologies (needle-shaped and
spherical) was studied by an in situ HT-ESEM method at
1340°C. La0.5Eu0.5PO4 pellets with high density $(99\%$ of
the theoretical density) were obtained for both precursor
powders by hot pressing. Analysis of XRD data collected for
the hot pressed pellets obtained from needle-shaped
precursors revealed preferential orientation of the grains
towards the (100) direction. Mechanical properties of the
hot pressed pellets were studied by the Vickers indentation
method. The dependence of microhardness and fracture
toughness on microstructure and texture was investigated.},
cin = {IEK-6},
ddc = {660},
cid = {I:(DE-Juel1)IEK-6-20101013},
pnm = {161 - Nuclear Waste Management (POF3-161) / BMBF-02NUK021A
- Verbundprojekt Conditioning: Grundlegende Untersuchungen
zur Immobilisierung langlebiger Radionuklide mittels Einbau
in endlagerrelevante Keramiken; Teilprojekt A
(BMBF-02NUK021A)},
pid = {G:(DE-HGF)POF3-161 / G:(DE-Juel1)BMBF-02NUK021A},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000414117500026},
doi = {10.1016/j.jeurceramsoc.2017.08.008},
url = {https://juser.fz-juelich.de/record/839910},
}