Contribution to a book FZJ-2017-08107

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Neutron Diffraction

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2017
Wiley-VCH Verlag GmbH & Co. KGaA Weinheim
ISBN: 978-3527325870, 9783527325870, 9783527691036 (electronic)

[Print] Handbook of solid state chemistry / Dronskowski, Richard ; Kikkawa, Shinichi ; Stein, Andreas , Weinheim : Wiley-VCH Verlag GmbH & Co. KGaA, 2017 Weinheim : Wiley-VCH Verlag GmbH & Co. KGaA Volume 3: Characterization, 77 - 108 ()

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Abstract: Neutron diffraction as an analytical tool in solid-state chemistry is briefly presented. We start by recalling a few characteristic properties of the neutron that make thermal neutrons a unique structural probe in solid-state science. The generation of neutrons, some fundamentals of neutron diffraction, concepts and components of instrumentation for powder as well as single-crystal neutron diffraction are briefly touched upon. A major part of this chapter deals with typical applications of neutron diffraction, among them being the study of hydrogen in crystals, the use of the peculiar diffraction contrast offered by neutrons to distinguish elements with similar atomic number, study of static disorder and thermal displacements in high-Tc superconductors, the superior precision of structural parameters obtained from neutron diffraction data, magnetic structures from neutron diffraction, complementary use of singlecrystal X-ray and neutron diffraction data to obtain bonding electron densities in crystals, and the determination of spatially resolved magnetization densities in solids. The last example contains spatially resolved in situ neutron diffraction on batteries.

Keyword(s): Energy (1st) ; Information and Communication (1st) ; Magnetic Materials (1st) ; Chemical Reactions and Advanced Materials (1st) ; Engineering, Industrial Materials and Processing (1st) ; Crystallography (2nd) ; Chemistry (2nd) ; Condensed Matter Physics (2nd) ; Industrial Application (2nd) ; Magnetism (2nd)

Classification:

Contributing Institute(s):
  1. JCNS-FRM-II (JCNS (München) ; Jülich Centre for Neutron Science JCNS (München) ; JCNS-FRM-II)
  2. Streumethoden (JCNS-2)
Research Program(s):
  1. 6G4 - Jülich Centre for Neutron Research (JCNS) (POF3-623) (POF3-623)
  2. 6G15 - FRM II / MLZ (POF3-6G15) (POF3-6G15)
Experiment(s):
  1. HEiDi: Single crystal diffractometer on hot source (SR9b)
  2. SPODI: High resolution powder diffractometer (SR8a)
  3. STRESS-SPEC: Materials science diffractometer (SR3)

Appears in the scientific report 2017
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OpenAccess
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 Record created 2017-12-06, last modified 2021-01-29