Journal Article FZJ-2018-02125

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Microstructure and Anisotropic Mechanical Properties of Freeze Dried SrTi0.75Fe0.25O3-δ for Oxygen Transport Membrane Substrates

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2018
Elsevier Science Amsterdam [u.a.]

Journal of the European Ceramic Society 38(7), 2774 - 2783 () [10.1016/j.jeurceramsoc.2018.02.014]

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Abstract: Hierarchically porous SrTi0.75Fe0.25O3-δ specimens were produced through a freeze drying procedure, which yielded a channel-like porosity, reaching a value of 32%. Compressive testing was used to determine apparent elastic modulus and fracture stresses in the transverse (out-of-plane) and longitudinal (in-plane) direction, revealing a strong dependence onto pore orientation. The lower mechanical stability in the in-plane direction appears to be associated with bending mode of the pore walls, being a result of a lower resistance to crack initiation. Acoustic emissions recorded during compressive tests indicated continuous damage of the pore walls before complete failure of the specimen, which could be also confirmed by complementary in-situ compressive tests in a scanning electronic microscope.

Classification:

Contributing Institute(s):
  1. Werkstoffsynthese und Herstellungsverfahren (IEK-1)
  2. Werkstoffstruktur und -eigenschaften (IEK-2)
Research Program(s):
  1. 111 - Efficient and Flexible Power Plants (POF3-111) (POF3-111)

Appears in the scientific report 2018
Database coverage:
Medline ; Current Contents - Engineering, Computing and Technology ; Current Contents - Physical, Chemical and Earth Sciences ; Ebsco Academic Search ; IF < 5 ; JCR ; SCOPUS ; Science Citation Index ; Science Citation Index Expanded ; Thomson Reuters Master Journal List ; Web of Science Core Collection
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Dokumenttypen > Aufsätze > Zeitschriftenaufsätze
Institutssammlungen > IMD > IMD-2
Institutssammlungen > IMD > IMD-1
Workflowsammlungen > Öffentliche Einträge
IEK > IEK-2
IEK > IEK-1
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