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@ARTICLE{Panchenko:863543,
author = {Panchenko, Olha and Arlt, Tobias and Manke, Ingo and
Müller, Martin and Stolten, Detlef and Lehnert, Werner},
title = {{S}ynchrotron {R}adiography for a {P}roton {E}xchange
{M}embrane ({PEM}) {E}lectrolyzer},
journal = {Fuel cells},
volume = {20},
number = {3},
issn = {1615-6846},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2019-03582},
pages = {300-306},
year = {2020},
abstract = {In‐plane synchrotron radiography with a resolution of a
few micrometers was applied to study transport processes
within a Proton Exchange Membrane (PEM) electrolyzer cell.
The degradation process of the catalyst layer, gas
production with bubble formation at the catalyst layer and
in the porous transport layer (PTL) was analyzed. From this,
a new cell design was developed that allows for high X‐ray
transmittances at the membrane plane in the in‐plane
viewing direction. During the measurement, a bubble growth
and movement was observed. Furthermore, a detachment of
catalytic material from the catalyst layer was detected.
Afterwards, a post mortem EDX analysis was conducted to
determine the position of the catalyst particles. Despite
Iridium being initially used as the anode catalyst and
platinum as the cathode catalyst, the EDX measurement
revealed Pt and Ir particles on both electrodes following
cell operation.},
cin = {IEK-3 / IEK-14},
ddc = {620},
cid = {I:(DE-Juel1)IEK-3-20101013 / I:(DE-Juel1)IEK-14-20191129},
pnm = {134 - Electrolysis and Hydrogen (POF3-134)},
pid = {G:(DE-HGF)POF3-134},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000513735500001},
doi = {10.1002/fuce.201900055},
url = {https://juser.fz-juelich.de/record/863543},
}