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000873679 1001_ $$0P:(DE-Juel1)166597$$aMishra, Tarini Prasad$$b0$$eCorresponding author
000873679 245__ $$aElectronic conductivity in gadolinium doped ceria under direct current as a trigger for flash sintering
000873679 260__ $$aAmsterdam [u.a.]$$bElsevier Science$$c2020
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000873679 520__ $$aIn this paper, we discuss the progression of flash sintering in 10mol% gadolinium-doped ceria specimens. Flash transition is correlated with the generation of n-type electronic conductivity in air under direct-current bias. Its origin is attributed to partial reduction of the material which propagates from the cathodic-to-anodic region. The phenomenon was observed, in-situ, by monitoring the development of electrochemical blackening during the incubation period of the flash-experiment. Anomalous features, including shift in the valence band edge, shrinkage of the band-gap and change in the oxidation state of Ce in flashed samples was confirmed by X-ray photoelectron spectroscopy and diffuse reflectance measurements.
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000873679 7001_ $$00000-0003-3064-9460$$aNeto, Rubens Roberto Ingraci$$b1
000873679 7001_ $$0P:(DE-HGF)0$$aSperanza, Giorgio$$b2
000873679 7001_ $$0P:(DE-HGF)0$$aQuaranta, Alberto$$b3
000873679 7001_ $$0P:(DE-HGF)0$$aSglavo, Vincenzo M.$$b4
000873679 7001_ $$00000-0001-8556-9797$$aRaj, Rishi$$b5
000873679 7001_ $$0P:(DE-Juel1)161591$$aGuillon, Olivier$$b6$$ufzj
000873679 7001_ $$0P:(DE-Juel1)129591$$aBram, Martin$$b7$$ufzj
000873679 7001_ $$00000-0002-4338-4177$$aBiesuz, Mattia$$b8$$eCorresponding author
000873679 773__ $$0PERI:(DE-600)2015843-9$$a10.1016/j.scriptamat.2020.01.007$$gVol. 179, p. 55 - 60$$p55 - 60$$tScripta materialia$$v179$$x1359-6462$$y2020
000873679 8564_ $$uhttps://juser.fz-juelich.de/record/873679/files/Manuscript_Blackening_Pre%20print.pdf$$yPublished on 2020-01-20. Available in OpenAccess from 2022-01-20.
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