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037 _ _ |a FZJ-2020-01933
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100 1 _ |a Ebner, Anna Sophie
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245 _ _ |a A Modified Electrochemical Nanoindentation Setup for Probing Hydrogen-Material Interaction Demonstrated on a Nickel-Based Alloy
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520 _ _ |a An electrochemical charging setup was implemented in a nanoindentation system to evaluate the sensitivity of technically relevant materials to hydrogen embrittlement. Corresponding changes in the nanomechanical properties such as the hardness, Young’s modulus and pop-in load can be measured and interpreted. A nickel-based alloy was examined in solution-annealed and aged condition. A hydrogen-induced hardness increase of 15% was measured for the solution-annealed sample. Aging the alloy leads to a reduced influence of hydrogen, lowering the hardness increase to 5%. For the solution-annealed sample, hydrogen charging-induced surface steps were observed and characterized with laser confocal microscopy and electron backscatter diffraction to reveal plastic deformation.
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700 1 _ |a Brinckmann, Steffen
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700 1 _ |a Plesiutschnig, Ernst
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700 1 _ |a Clemens, Helmut
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700 1 _ |a Pippan, Reinhard
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700 1 _ |a Maier-Kiener, Verena
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773 _ _ |a 10.1007/s11837-020-04104-9
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856 4 _ |u https://juser.fz-juelich.de/record/875302/files/Ebner2020_Article_AModifiedElectrochemicalNanoin.pdf
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