Journal Article FZJ-2020-01933

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A Modified Electrochemical Nanoindentation Setup for Probing Hydrogen-Material Interaction Demonstrated on a Nickel-Based Alloy

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2020
TMS [S.l.]

JOM 72(5), 2020 - 2029 () [10.1007/s11837-020-04104-9]

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Abstract: An electrochemical charging setup was implemented in a nanoindentation system to evaluate the sensitivity of technically relevant materials to hydrogen embrittlement. Corresponding changes in the nanomechanical properties such as the hardness, Young’s modulus and pop-in load can be measured and interpreted. A nickel-based alloy was examined in solution-annealed and aged condition. A hydrogen-induced hardness increase of 15% was measured for the solution-annealed sample. Aging the alloy leads to a reduced influence of hydrogen, lowering the hardness increase to 5%. For the solution-annealed sample, hydrogen charging-induced surface steps were observed and characterized with laser confocal microscopy and electron backscatter diffraction to reveal plastic deformation.

Classification:

Contributing Institute(s):
  1. Werkstoffstruktur und -eigenschaften (IEK-2)
Research Program(s):
  1. 113 - Methods and Concepts for Material Development (POF3-113) (POF3-113)
  2. 1241 - Gas turbines (POF4-124) (POF4-124)

Appears in the scientific report 2020
Database coverage:
Medline ; Creative Commons Attribution CC BY 4.0 ; OpenAccess ; Clarivate Analytics Master Journal List ; Current Contents - Engineering, Computing and Technology ; IF < 5 ; JCR ; SCOPUS ; Science Citation Index ; Science Citation Index Expanded ; Web of Science Core Collection
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Institute Collections > IMD > IMD-1
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Open Access

 Record created 2020-05-11, last modified 2024-07-11