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| 001 | 877638 | ||
| 005 | 20240712113053.0 | ||
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| 100 | 1 | _ | |a Ye, Ruijie |0 P:(DE-Juel1)176118 |b 0 |u fzj |
| 245 | _ | _ | |a Water-based fabrication of garnet-based solid electrolyte separators for solid-state lithium batteries |
| 260 | _ | _ | |a Cambridge |c 2020 |b RSC |
| 336 | 7 | _ | |a article |2 DRIVER |
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| 520 | _ | _ | |a Garnet-type Li7La3Zr2O12 (LLZ) is regarded as a promising oxide-based solid electrolyte (SE) for solid-state lithium batteries (SSLBs) or other advanced Li-battery concepts like Li–air or Li–S batteries. A thin free-standing LLZ sheet can be fabricated by tape-casting and used e.g. as separators in SSLBs, since tape casting is an industrially established process and enables large-scale production of such SEs. However, organic solvents and additives employed in conventional slurry recipes for tape-casting give rise to health and safety concerns and also cause a high cost for solvent recovery. Hence, development of a green, water-based processing route can reduce both manufacturing costs and environmental footprint. In this work, we developed a tape-casting process for LLZ SEs using water as solvent, the water-soluble biopolymer methylcellulose as binder and other eco-friendly polymers as plasticizers. Although a Li+/H+ exchange takes place during our procedure, we demonstrate that the Li+/H+ exchange reaction is reversible in our procedure and results in the formation of stoichiometric cubic LLZ at the end. The obtained free-standing LLZ sheets with thickness of 150 μm and relative density of approx. 90% offer an ionic conductivity of 0.15 mS cm−1 at room temperature. We thereby prove that it is feasible to use water as dispersion medium and eco-friendly polymer additives for the fabrication of thin garnet-based SE layers. |
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| 700 | 1 | _ | |a Tsai, Chih-Long |0 P:(DE-Juel1)156244 |b 1 |
| 700 | 1 | _ | |a Ihrig, Martin |0 P:(DE-Juel1)174298 |b 2 |u fzj |
| 700 | 1 | _ | |a Sevinc, Serkan |0 P:(DE-Juel1)176429 |b 3 |u fzj |
| 700 | 1 | _ | |a Rosen, Melanie |0 P:(DE-Juel1)173936 |b 4 |u fzj |
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| 700 | 1 | _ | |a Figgemeier, Egbert |0 P:(DE-Juel1)165182 |b 7 |e Corresponding author |u fzj |
| 700 | 1 | _ | |a Finsterbusch, Martin |0 P:(DE-Juel1)145623 |b 8 |e Corresponding author |
| 773 | _ | _ | |a 10.1039/D0GC01009J |g p. 10.1039.D0GC01009J |0 PERI:(DE-600)2006274-6 |n 15 |p 4952-4961 |t Green chemistry |v 22 |y 2020 |x 1463-9262 |
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