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@ARTICLE{Hao:878192,
author = {Hao, Yucheng and Alekseev, Evgeny and Klepov, Vladislav V.
and Yu, Na},
title = {{S}tructural {V}ariations in {C}omplex {S}odium {T}horium
{A}rsenates},
journal = {European journal of inorganic chemistry},
volume = {2020},
number = {33},
issn = {1434-1948},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2020-02680},
pages = {3187-3193},
year = {2020},
note = {Arbeit ist am IEK-6 entstanden},
abstract = {Three new sodium thorium arsenates, Na5Th4(AsO4)7 (1 ),
Na5Th(AsO4)3 (2 ), and Na4Th(As2O7)2 (3 ) were synthesized
via a high temperature route and their structures and
optical properties were studied. Compound 1 adopts a
three‐dimensional structure that consists of tetrameric
fundamental building blocks (FBBs) [Th4(AsO4)7]5–, which
are constructed by ThO8 and ThO9 polyhedra. The structures
of 2 and 3 are based on open frameworks with channels
running along the a or c axes, respectively, which are
occupied by Na cations. Structural relations between the
structures of 2 and 3 have been discussed regarding their
composition. In contrast to the other two compounds, the
arsenate anions in the structure of 2 play role of bridging
ligands and do not connect more than two Th atoms. Owing to
this, the underlying net of this compound contains only Th
nodes has a lon topology. The Raman spectra of 1 and 2
contain similar peaks due to As–O vibrations of AsO4
groups, while the Raman spectrum of 3 differs significantly
owing to the presence of As–O–As bridging group in
As2O74– anions.},
cin = {IEK-9 / IEK-6},
ddc = {540},
cid = {I:(DE-Juel1)IEK-9-20110218 / I:(DE-Juel1)IEK-6-20101013},
pnm = {131 - Electrochemical Storage (POF3-131) / 161 - Nuclear
Waste Management (POF3-161)},
pid = {G:(DE-HGF)POF3-131 / G:(DE-HGF)POF3-161},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000563891900001},
doi = {10.1002/ejic.202000492},
url = {https://juser.fz-juelich.de/record/878192},
}