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@ARTICLE{Lin:878369,
author = {Lin, Jingjing and Korte, C.},
title = {{PBI}‐type {P}olymers and {A}cidic {P}roton {C}onducting
{I}onic {L}iquids – {C}onductivity and {M}olecular
{I}nteractions},
journal = {Fuel cells},
volume = {20},
number = {4},
issn = {1615-6854},
address = {Weinheim},
publisher = {Wiley-VCH},
reportid = {FZJ-2020-02809},
pages = {461-468},
year = {2020},
abstract = {Proton conducting ionic liquids (PILs) are discussed as new
electrolytes for the use as non‐aqueous electrolytes at
operation temperatures above 100 °C. During fuel cell
operation the presence of significant amounts of residual
water is unavoidable. The highly Brønsted‐acidic PIL
2‐Sulfoethylmethylammonum triflate [2‐Sema][TfO] is able
to perform fast proton exchange processes with H2O,
resulting from 1H‐NMR and pulsed field gradient
(PFG)/diffusion ordered spectroscopy (DOSY) self‐diffusion
measurements. Proton conduction takes place by a vehicle
mechanism via PIL cations or H3O+, but also by a cooperative
mechanism involving both species. Thus, highly
Brønsted‐acidic PILs are promising candidates for the use
as non‐aqueous electrolytes. To use [2‐Sema][TfO] as
electrolyte in a proton electrolyte fuel cell (PEFC) it has
to be immobilized in a host polymer. There is a (slow)
uptake of the PIL by polybenzimidazole (PBI) up to a weight
increase of $∼130\%,$ due to a swelling process. A
protonation of the basic imidazole moieties takes place. NMR
analysis was applied to elucidate the molecular interactions
between PBI, PIL, and residual water. Proton exchange,
respectively an interaction between the polar groups and
water can be observed in spectra, indicating a network of
H‐bonds in doped PBI. Therefore, highly acidic PILs are
promising candidates for the use as non‐aqueous
electrolytes.},
cin = {IEK-14},
ddc = {620},
cid = {I:(DE-Juel1)IEK-14-20191129},
pnm = {135 - Fuel Cells (POF3-135)},
pid = {G:(DE-HGF)POF3-135},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000563058600009},
doi = {10.1002/fuce.201900201},
url = {https://juser.fz-juelich.de/record/878369},
}