000887742 001__ 887742
000887742 005__ 20230310131355.0
000887742 0247_ $$2doi$$a10.1016/j.ultramic.2020.113166
000887742 0247_ $$2ISSN$$a0304-3991
000887742 0247_ $$2ISSN$$a1879-2723
000887742 0247_ $$2Handle$$a2128/26559
000887742 0247_ $$2altmetric$$aaltmetric:94848697
000887742 0247_ $$2pmid$$a33227698
000887742 0247_ $$2WOS$$aWOS:000600307200002
000887742 037__ $$aFZJ-2020-04399
000887742 082__ $$a570
000887742 1001_ $$0P:(DE-Juel1)166383$$aYuan, Yu$$b0
000887742 245__ $$aExtraction of 3D quantitative maps using EDS-STEM tomography and HAADF-EDS bimodal tomography
000887742 260__ $$aAmsterdam$$bElsevier Science$$c2020
000887742 3367_ $$2DRIVER$$aarticle
000887742 3367_ $$2DataCite$$aOutput Types/Journal article
000887742 3367_ $$0PUB:(DE-HGF)16$$2PUB:(DE-HGF)$$aJournal Article$$bjournal$$mjournal$$s1608106278_1985
000887742 3367_ $$2BibTeX$$aARTICLE
000887742 3367_ $$2ORCID$$aJOURNAL_ARTICLE
000887742 3367_ $$00$$2EndNote$$aJournal Article
000887742 520__ $$aElectron tomography has been widely applied to three-dimensional (3D) morphology characterization and chemical analysis at the nanoscale. A HAADF-EDS bimodal tomographic (HEBT) reconstruction technique has been developed to extract high resolution element-specific information. However, the reconstructed elemental maps cannot be directly converted to quantitative compositional information. In this work, we propose a quantification approach for obtaining elemental weight fraction maps from the HEBT reconstruction technique using the physical parameters extracted from a Monte Carlo code, MC X-ray. A similar quantification approach is proposed for the EDS-STEM tomographic reconstruction. The performance of the two quantitative reconstruction methods, using the simultaneous iterative reconstruction technique, are evaluated and compared for a simulated dataset of a two-dimensional phantom sample. The effects of the reconstruction parameters including the number of iterations and the weight of the HAADF signal are discussed. Finally, the two approaches are applied to an experimental dataset to show the 3D structure and quantitative elemental maps of a particle of flux melted metal-organic framework glass.
000887742 536__ $$0G:(DE-HGF)POF3-143$$a143 - Controlling Configuration-Based Phenomena (POF3-143)$$cPOF3-143$$fPOF III$$x0
000887742 536__ $$0G:(GEPRIS)257727131$$aDFG project 257727131 - Nanoskalige Pt Legierungselektrokatalysatoren mit definierter Morphologie: Synthese, Electrochemische Analyse, und ex-situ/in-situ Transmissionselektronenmikroskopische (TEM) Studien (257727131)$$c257727131$$x1
000887742 588__ $$aDataset connected to CrossRef
000887742 7001_ $$0P:(DE-Juel1)168372$$aMacArthur, Katherine E.$$b1$$eCorresponding author
000887742 7001_ $$0P:(DE-HGF)0$$aCollins, Sean M.$$b2
000887742 7001_ $$0P:(DE-HGF)0$$aBrodusch, Nicolas$$b3
000887742 7001_ $$0P:(DE-HGF)0$$aVoisard, Frédéric$$b4
000887742 7001_ $$0P:(DE-Juel1)144121$$aDunin-Borkowski, Rafal E.$$b5
000887742 7001_ $$0P:(DE-HGF)0$$aGauvin, Raynald$$b6$$eCorresponding author
000887742 773__ $$0PERI:(DE-600)1479043-9$$a10.1016/j.ultramic.2020.113166$$gp. 113166 -$$p113166 -$$tUltramicroscopy$$v220$$x0304-3991$$y2020
000887742 8564_ $$uhttps://juser.fz-juelich.de/record/887742/files/1-s2.0-S0304399120303090-main.pdf
000887742 8564_ $$uhttps://juser.fz-juelich.de/record/887742/files/Extraction_of_3D_quantitative_maps.pdf$$yPublished on 2020-11-09. Available in OpenAccess from 2022-11-09.
000887742 8564_ $$uhttps://juser.fz-juelich.de/record/887742/files/Extraction_of_3D_quantitative_maps.pdf?subformat=pdfa$$xpdfa$$yPublished on 2020-11-09. Available in OpenAccess from 2022-11-09.
000887742 909CO $$ooai:juser.fz-juelich.de:887742$$pdnbdelivery$$pdriver$$pVDB$$popen_access$$popenaire
000887742 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)168372$$aForschungszentrum Jülich$$b1$$kFZJ
000887742 9101_ $$0I:(DE-588b)5008462-8$$6P:(DE-Juel1)144121$$aForschungszentrum Jülich$$b5$$kFZJ
000887742 9131_ $$0G:(DE-HGF)POF3-143$$1G:(DE-HGF)POF3-140$$2G:(DE-HGF)POF3-100$$3G:(DE-HGF)POF3$$4G:(DE-HGF)POF$$aDE-HGF$$bEnergie$$lFuture Information Technology - Fundamentals, Novel Concepts and Energy Efficiency (FIT)$$vControlling Configuration-Based Phenomena$$x0
000887742 9141_ $$y2020
000887742 915__ $$0StatID:(DE-HGF)0200$$2StatID$$aDBCoverage$$bSCOPUS$$d2020-09-02
000887742 915__ $$0StatID:(DE-HGF)0160$$2StatID$$aDBCoverage$$bEssential Science Indicators$$d2020-09-02
000887742 915__ $$0StatID:(DE-HGF)1050$$2StatID$$aDBCoverage$$bBIOSIS Previews$$d2020-09-02
000887742 915__ $$0StatID:(DE-HGF)1190$$2StatID$$aDBCoverage$$bBiological Abstracts$$d2020-09-02
000887742 915__ $$0StatID:(DE-HGF)0600$$2StatID$$aDBCoverage$$bEbsco Academic Search$$d2020-09-02
000887742 915__ $$0LIC:(DE-HGF)CCBYNCND4$$2HGFVOC$$aCreative Commons Attribution-NonCommercial-NoDerivs CC BY-NC-ND 4.0
000887742 915__ $$0StatID:(DE-HGF)0530$$2StatID$$aEmbargoed OpenAccess
000887742 915__ $$0StatID:(DE-HGF)0100$$2StatID$$aJCR$$bULTRAMICROSCOPY : 2018$$d2020-09-02
000887742 915__ $$0StatID:(DE-HGF)1030$$2StatID$$aDBCoverage$$bCurrent Contents - Life Sciences$$d2020-09-02
000887742 915__ $$0StatID:(DE-HGF)0113$$2StatID$$aWoS$$bScience Citation Index Expanded$$d2020-09-02
000887742 915__ $$0StatID:(DE-HGF)0150$$2StatID$$aDBCoverage$$bWeb of Science Core Collection$$d2020-09-02
000887742 915__ $$0StatID:(DE-HGF)9900$$2StatID$$aIF < 5$$d2020-09-02
000887742 915__ $$0StatID:(DE-HGF)0030$$2StatID$$aPeer Review$$bASC$$d2020-09-02
000887742 915__ $$0StatID:(DE-HGF)1150$$2StatID$$aDBCoverage$$bCurrent Contents - Physical, Chemical and Earth Sciences$$d2020-09-02
000887742 915__ $$0StatID:(DE-HGF)0300$$2StatID$$aDBCoverage$$bMedline$$d2020-09-02
000887742 915__ $$0StatID:(DE-HGF)0420$$2StatID$$aNationallizenz$$d2020-09-02$$wger
000887742 915__ $$0StatID:(DE-HGF)0199$$2StatID$$aDBCoverage$$bClarivate Analytics Master Journal List$$d2020-09-02
000887742 920__ $$lyes
000887742 9201_ $$0I:(DE-Juel1)ER-C-1-20170209$$kER-C-1$$lPhysik Nanoskaliger Systeme$$x0
000887742 980__ $$ajournal
000887742 980__ $$aVDB
000887742 980__ $$aUNRESTRICTED
000887742 980__ $$aI:(DE-Juel1)ER-C-1-20170209
000887742 9801_ $$aFullTexts