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@ARTICLE{Yuan:887742,
      author       = {Yuan, Yu and MacArthur, Katherine E. and Collins, Sean M.
                      and Brodusch, Nicolas and Voisard, Frédéric and
                      Dunin-Borkowski, Rafal E. and Gauvin, Raynald},
      title        = {{E}xtraction of 3{D} quantitative maps using {EDS}-{STEM}
                      tomography and {HAADF}-{EDS} bimodal tomography},
      journal      = {Ultramicroscopy},
      volume       = {220},
      issn         = {0304-3991},
      address      = {Amsterdam},
      publisher    = {Elsevier Science},
      reportid     = {FZJ-2020-04399},
      pages        = {113166 -},
      year         = {2020},
      abstract     = {Electron tomography has been widely applied to
                      three-dimensional (3D) morphology characterization and
                      chemical analysis at the nanoscale. A HAADF-EDS bimodal
                      tomographic (HEBT) reconstruction technique has been
                      developed to extract high resolution element-specific
                      information. However, the reconstructed elemental maps
                      cannot be directly converted to quantitative compositional
                      information. In this work, we propose a quantification
                      approach for obtaining elemental weight fraction maps from
                      the HEBT reconstruction technique using the physical
                      parameters extracted from a Monte Carlo code, MC X-ray. A
                      similar quantification approach is proposed for the EDS-STEM
                      tomographic reconstruction. The performance of the two
                      quantitative reconstruction methods, using the simultaneous
                      iterative reconstruction technique, are evaluated and
                      compared for a simulated dataset of a two-dimensional
                      phantom sample. The effects of the reconstruction parameters
                      including the number of iterations and the weight of the
                      HAADF signal are discussed. Finally, the two approaches are
                      applied to an experimental dataset to show the 3D structure
                      and quantitative elemental maps of a particle of flux melted
                      metal-organic framework glass.},
      cin          = {ER-C-1},
      ddc          = {570},
      cid          = {I:(DE-Juel1)ER-C-1-20170209},
      pnm          = {143 - Controlling Configuration-Based Phenomena (POF3-143)
                      / DFG project 257727131 - Nanoskalige Pt
                      Legierungselektrokatalysatoren mit definierter Morphologie:
                      Synthese, Electrochemische Analyse, und ex-situ/in-situ
                      Transmissionselektronenmikroskopische (TEM) Studien
                      (257727131)},
      pid          = {G:(DE-HGF)POF3-143 / G:(GEPRIS)257727131},
      typ          = {PUB:(DE-HGF)16},
      pubmed       = {33227698},
      UT           = {WOS:000600307200002},
      doi          = {10.1016/j.ultramic.2020.113166},
      url          = {https://juser.fz-juelich.de/record/887742},
}