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000890389 1001_ $$0P:(DE-Juel1)176806$$aNur, Khushnuda$$b0$$eCorresponding author$$ufzj
000890389 245__ $$aInfluence of powder characteristics on cold sintering of nano-sized ZnO with density above 99 %
000890389 260__ $$aAmsterdam [u.a.]$$bElsevier Science$$c2021
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000890389 520__ $$aCold sintering parameters such as, temperature, pressure, aqueous phase, heating rate and dwelling time has been widely discussed in the literature but the role of starting powder with respective microstructure development is mostly overlooked. There is a need for understanding the effect of powder agglomerates and the role of inter particle friction on the densification behavior during cold sintering process. Present study encompasses investigation and optimization of these parameters for ZnO which enabled > 99 % of relative density with grain sizes below 200 nm. Additionally, role of external atmosphere was also studied to investigate its impact on densification during the process. All cold sintering experiments were carried out in a FAST/SPS device for studying aqueous phase evaporation and ensuring the reproducibility of process parameters. Microstructure characterization (scanning and transmission electron microscopy) showed – without any post heat treatment– defect free grain boundary structure opposite to what documented by previous studies.
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000890389 7001_ $$0P:(DE-Juel1)166597$$aMishra, Tarini Prasad$$b1
000890389 7001_ $$0P:(DE-HGF)0$$aSilva, João Gustavo Pereira da$$b2
000890389 7001_ $$0P:(DE-Juel1)162271$$aGonzalez-Julian, Jesus$$b3
000890389 7001_ $$0P:(DE-Juel1)129591$$aBram, Martin$$b4$$ufzj
000890389 7001_ $$0P:(DE-Juel1)161591$$aGuillon, Olivier$$b5$$ufzj
000890389 773__ $$0PERI:(DE-600)2013983-4$$a10.1016/j.jeurceramsoc.2020.11.007$$gVol. 41, no. 4, p. 2648 - 2662$$n4$$p2648 - 2662$$tJournal of the European Ceramic Society$$v41$$x0955-2219$$y2021
000890389 8564_ $$uhttps://juser.fz-juelich.de/record/890389/files/JUCER%20J%20Europ%20Ceram%20Soc_Nur%20et%20al_Manuscript_revisions%20-%20JUCER.pdf$$yPublished on 2020-11-11. Available in OpenAccess from 2021-11-11.
000890389 8564_ $$uhttps://juser.fz-juelich.de/record/890389/files/JUCER%20J%20Europ%20Ceram%20Soc_Nur%20et%20al_revised%20supplementary%20information%20.pdf$$yPublished on 2020-11-11. Available in OpenAccess from 2021-11-11.
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