guest ::
| Home > Workflow collections > Publication Charges > Optimizing Experimental Conditions for Accurate Quantitative Energy-Dispersive X-ray Analysis of Interfaces at the Atomic Scale > print |
| Home > Workflow collections > Publication Charges > Optimizing Experimental Conditions for Accurate Quantitative Energy-Dispersive X-ray Analysis of Interfaces at the Atomic Scale > print |
| 001 | 891572 | ||
| 005 | 20240610120304.0 | ||
| 024 | 7 | _ | |a 10.1017/S1431927621000246 |2 doi |
| 024 | 7 | _ | |a 1431-9276 |2 ISSN |
| 024 | 7 | _ | |a 1435-8115 |2 ISSN |
| 024 | 7 | _ | |a 2128/28159 |2 Handle |
| 024 | 7 | _ | |a altmetric:104677530 |2 altmetric |
| 024 | 7 | _ | |a 33843542 |2 pmid |
| 024 | 7 | _ | |a WOS:000664532400007 |2 WOS |
| 037 | _ | _ | |a FZJ-2021-01597 |
| 082 | _ | _ | |a 500 |
| 100 | 1 | _ | |a MacArthur, Katherine E. |0 P:(DE-Juel1)168372 |b 0 |e Corresponding author |
| 245 | _ | _ | |a Optimizing Experimental Conditions for Accurate Quantitative Energy-Dispersive X-ray Analysis of Interfaces at the Atomic Scale |
| 260 | _ | _ | |a New York, NY |c 2021 |b Cambridge University Press |
| 336 | 7 | _ | |a article |2 DRIVER |
| 336 | 7 | _ | |a Output Types/Journal article |2 DataCite |
| 336 | 7 | _ | |a Journal Article |b journal |m journal |0 PUB:(DE-HGF)16 |s 1626178012_14697 |2 PUB:(DE-HGF) |
| 336 | 7 | _ | |a ARTICLE |2 BibTeX |
| 336 | 7 | _ | |a JOURNAL_ARTICLE |2 ORCID |
| 336 | 7 | _ | |a Journal Article |0 0 |2 EndNote |
| 520 | _ | _ | |a The invention of silicon drift detectors has resulted in an unprecedented improvement in detection efficiency for energy-dispersive X-ray (EDX) spectroscopy in the scanning transmission electron microscope. The result is numerous beautiful atomic-scale maps, which provide insights into the internal structure of a variety of materials. However, the task still remains to understand exactly where the X-ray signal comes from and how accurately it can be quantified. Unfortunately, when crystals are aligned with a low-order zone axis parallel to the incident beam direction, as is necessary for atomic-resolution imaging, the electron beam channels. When the beam becomes localized in this way, the relationship between the concentration of a particular element and its spectroscopic X-ray signal is generally nonlinear. Here, we discuss the combined effect of both spatial integration and sample tilt for ameliorating the effects of channeling and improving the accuracy of EDX quantification. Both simulations and experimental results will be presented for a perovskite-based oxide interface. We examine how the scattering and spreading of the electron beam can lead to erroneous interpretation of interface compositions, and what approaches can be made to improve our understanding of the underlying atomic structure. |
| 536 | _ | _ | |a 535 - Materials Information Discovery (POF4-535) |0 G:(DE-HGF)POF4-535 |c POF4-535 |x 0 |f POF IV |
| 536 | _ | _ | |a DFG project 257727131 - Nanoskalige Pt Legierungselektrokatalysatoren mit definierter Morphologie: Synthese, Electrochemische Analyse, und ex-situ/in-situ Transmissionselektronenmikroskopische (TEM) Studien (257727131) |0 G:(GEPRIS)257727131 |c 257727131 |x 1 |
| 588 | _ | _ | |a Dataset connected to CrossRef |
| 700 | 1 | _ | |a Yankovich, Andrew B. |0 P:(DE-HGF)0 |b 1 |
| 700 | 1 | _ | |a Béché, Armand |0 P:(DE-HGF)0 |b 2 |
| 700 | 1 | _ | |a Luysberg, Martina |0 P:(DE-Juel1)130811 |b 3 |u fzj |
| 700 | 1 | _ | |a Brown, Hamish G. |0 P:(DE-HGF)0 |b 4 |
| 700 | 1 | _ | |a Findlay, Scott D. |0 P:(DE-HGF)0 |b 5 |
| 700 | 1 | _ | |a Heggen, Marc |0 P:(DE-Juel1)130695 |b 6 |u fzj |
| 700 | 1 | _ | |a Allen, Leslie J. |0 P:(DE-HGF)0 |b 7 |
| 773 | _ | _ | |a 10.1017/S1431927621000246 |g p. 1 - 15 |0 PERI:(DE-600)1481716-0 |n 3 |p 528 |t Microscopy and microanalysis |v 27 |y 2021 |x 1431-9276 |
| 856 | 4 | _ | |u https://juser.fz-juelich.de/record/891572/files/Invoice_APC600204312.pdf |
| 856 | 4 | _ | |y OpenAccess |u https://juser.fz-juelich.de/record/891572/files/optimizing-experimental-conditions-for-accurate-quantitative-energy-dispersive-x-ray-analysis-of-interfaces-at-the-atomic-scale-1.pdf |
| 909 | C | O | |o oai:juser.fz-juelich.de:891572 |p openaire |p open_access |p OpenAPC |p driver |p VDB |p openCost |p dnbdelivery |
| 910 | 1 | _ | |a Forschungszentrum Jülich |0 I:(DE-588b)5008462-8 |k FZJ |b 0 |6 P:(DE-Juel1)168372 |
| 910 | 1 | _ | |a Forschungszentrum Jülich |0 I:(DE-588b)5008462-8 |k FZJ |b 3 |6 P:(DE-Juel1)130811 |
| 910 | 1 | _ | |a Forschungszentrum Jülich |0 I:(DE-588b)5008462-8 |k FZJ |b 6 |6 P:(DE-Juel1)130695 |
| 913 | 1 | _ | |a DE-HGF |b Key Technologies |l Materials Systems Engineering |1 G:(DE-HGF)POF4-530 |0 G:(DE-HGF)POF4-535 |3 G:(DE-HGF)POF4 |2 G:(DE-HGF)POF4-500 |4 G:(DE-HGF)POF |v Materials Information Discovery |x 0 |
| 913 | 0 | _ | |a DE-HGF |b Energie |l Future Information Technology - Fundamentals, Novel Concepts and Energy Efficiency (FIT) |1 G:(DE-HGF)POF3-140 |0 G:(DE-HGF)POF3-143 |3 G:(DE-HGF)POF3 |2 G:(DE-HGF)POF3-100 |4 G:(DE-HGF)POF |v Controlling Configuration-Based Phenomena |x 0 |
| 914 | 1 | _ | |y 2021 |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)0200 |2 StatID |b SCOPUS |d 2021-02-05 |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)0160 |2 StatID |b Essential Science Indicators |d 2021-02-05 |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)1050 |2 StatID |b BIOSIS Previews |d 2021-02-05 |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)1190 |2 StatID |b Biological Abstracts |d 2021-02-05 |
| 915 | _ | _ | |a Creative Commons Attribution CC BY 4.0 |0 LIC:(DE-HGF)CCBY4 |2 HGFVOC |
| 915 | _ | _ | |a OpenAccess |0 StatID:(DE-HGF)0510 |2 StatID |
| 915 | _ | _ | |a JCR |0 StatID:(DE-HGF)0100 |2 StatID |b MICROSC MICROANAL : 2019 |d 2021-02-05 |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)1030 |2 StatID |b Current Contents - Life Sciences |d 2021-02-05 |
| 915 | _ | _ | |a WoS |0 StatID:(DE-HGF)0113 |2 StatID |b Science Citation Index Expanded |d 2021-02-05 |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)0150 |2 StatID |b Web of Science Core Collection |d 2021-02-05 |
| 915 | _ | _ | |a IF < 5 |0 StatID:(DE-HGF)9900 |2 StatID |d 2021-02-05 |
| 915 | _ | _ | |a Allianz-Lizenz / DFG |0 StatID:(DE-HGF)0400 |2 StatID |d 2021-02-05 |w ger |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)1150 |2 StatID |b Current Contents - Physical, Chemical and Earth Sciences |d 2021-02-05 |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)0300 |2 StatID |b Medline |d 2021-02-05 |
| 915 | _ | _ | |a Nationallizenz |0 StatID:(DE-HGF)0420 |2 StatID |d 2021-02-05 |w ger |
| 915 | _ | _ | |a DBCoverage |0 StatID:(DE-HGF)0199 |2 StatID |b Clarivate Analytics Master Journal List |d 2021-02-05 |
| 920 | _ | _ | |l yes |
| 920 | 1 | _ | |0 I:(DE-Juel1)PGI-5-20110106 |k PGI-5 |l Mikrostrukturforschung |x 0 |
| 920 | 1 | _ | |0 I:(DE-Juel1)ER-C-1-20170209 |k ER-C-1 |l Physik Nanoskaliger Systeme |x 1 |
| 980 | 1 | _ | |a APC |
| 980 | 1 | _ | |a FullTexts |
| 980 | _ | _ | |a journal |
| 980 | _ | _ | |a VDB |
| 980 | _ | _ | |a UNRESTRICTED |
| 980 | _ | _ | |a I:(DE-Juel1)PGI-5-20110106 |
| 980 | _ | _ | |a I:(DE-Juel1)ER-C-1-20170209 |
| 980 | _ | _ | |a APC |
| 981 | _ | _ | |a I:(DE-Juel1)ER-C-1-20170209 |
| Library | Collection | CLSMajor | CLSMinor | Language | Author |
|---|