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@ARTICLE{Stolz:891849,
author = {Stolz, Lukas and Homann, Gerrit and Winter, Martin and
Kasnatscheew, Johannes},
title = {{R}ealizing poly(ethylene oxide) as a polymer for solid
electrolytes in high voltage lithium batteries via simple
modification of the cell setup},
journal = {Materials advances},
volume = {2},
number = {10},
issn = {2633-5409},
address = {Cambridge},
publisher = {Royal Society of Chemistry},
reportid = {FZJ-2021-01769},
pages = {3251-3256},
year = {2021},
abstract = {Pure, i.e., linear poly(ethylene oxide)-based solid polymer
electrolyte (PEO-based SPE) as a common benchmark system for
Li metal batteries (LMBs) is frequently assumed to be
unsuitable for high voltage applications e.g., with
LiNi0.6Mn0.2Co0.2O2 (NMC622)-based cathodes. In fact, a
destructive failure appears immediately after cell
operation, seen by a random-like “voltage noise” during
charge, rendering continuous charge/discharge cycling in
e.g., NMC622||Li cells not possible. Counterintuitively,
this failure is a result of short-circuits in the course of
e.g., Li dendrite penetration. It is shown that the distance
between the electrodes plays a crucial role. This failure is
more likely with a lower distance, particularly when the SPE
is mechanically prone to shrinkage, for example at higher
temperatures as systematically revealed by mechanical
compression tests. Additionally, the active mass loading has
a crucial impact on short circuits, and thus the “voltage
noise” failure, as well. An effective and practically
simple solution to realize cell operation with a PEO-based
SPE is the incorporation of a spacer between the electrodes.
This modification prevents the detrimental shrinkage and
enables charge/discharge cycling performance in NMC622||Li
cells with a defined and constant electrode distance, thus
without voltage noise, and finally fulfills a reasonable
benchmark for systematic $R\&D$ with specific capacities
above 150 mA h g−1 even at 40 °C.},
cin = {IEK-12},
ddc = {540},
cid = {I:(DE-Juel1)IEK-12-20141217},
pnm = {121 - Photovoltaik und Windenergie (POF4-121)},
pid = {G:(DE-HGF)POF4-121},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000639982700001},
doi = {10.1039/D1MA00009H},
url = {https://juser.fz-juelich.de/record/891849},
}