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@ARTICLE{Jalalpoor:893908,
author = {Jalalpoor, Daniel and Göhl, Daniel and Paciok, Paul and
Heggen, Marc and Knossalla, Johannes and Radev, Ivan and
Peinecke, Volker and Weidenthaler, Claudia and Mayrhofer,
Karl J. J. and Ledendecker, Marc and Schüth, Ferdi},
title = {{T}he {I}mpact of {A}ntimony on the {P}erformance of
{A}ntimony {D}oped {T}in {O}xide {S}upported {P}latinum for
the {O}xygen {R}eduction {R}eaction},
journal = {Journal of the Electrochemical Society},
volume = {168},
number = {2},
issn = {1945-7111},
address = {Bristol},
publisher = {IOP Publishing},
reportid = {FZJ-2021-02920},
pages = {024502 -},
year = {2021},
abstract = {Daniel Jalalpoor, Daniel Göhl, Paul Paciok, Marc Heggen,
Johannes Knossalla, Ivan Radev, Volker Peinecke, Claudia
Weidenthaler, Karl J. J. Mayrhofer, “The Impact of
Antimony on the Performance of Antimony Doped Tin Oxide
Supported Platinum for the Oxygen Reduction Reaction”, J.
Electrochem. Soc. 168, (2021) 024502
https://doi.org/10.1149/1945-7111/abd830 Abstract:Antimony
doped tin oxide (ATO) supported platinum nanoparticles are
considered a more stable replacement for conventional carbon
supported platinum materials for the oxygen reduction
reaction. However, the interplay of antimony, tin and
platinum and its impact on the catalytic activity and
durability has only received minor attention. This is partly
due to difficulties in the preparation of morphology- and
surface-area-controlled antimony-doped tin oxide materials.
The presented study sheds light onto catalyst–support
interaction on a fundamental level, specifically between
platinum as a catalyst and ATO as a support material. By
using a previously described hard-templating method, a
series of morphology controlled ATO support materials for
platinum nanoparticles with different antimony doping
concentrations were prepared. Compositional and
morphological changes before and during accelerated stress
tests are monitored, and underlying principles of
deactivation, dissolution and catalytic performance are
elaborated. We demonstrate that mobilized antimony species
and strong metal support interactions lead to Pt/Sb alloy
formation as well as partially blocking of active sites.
This has adverse consequences on the accessible platinum
surface area, and affects negatively the catalytic
performance of platinum. Operando time-resolved dissolution
experiments uncover the potential boundary conditions at
which antimony dissolution can be effectively suppressed and
how platinum influences the dissolution behavior of the
support.},
cin = {ER-C-1},
ddc = {660},
cid = {I:(DE-Juel1)ER-C-1-20170209},
pnm = {5351 - Platform for Correlative, In Situ and Operando
Characterization (POF4-535)},
pid = {G:(DE-HGF)POF4-5351},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000616613500001},
doi = {10.1149/1945-7111/abd830},
url = {https://juser.fz-juelich.de/record/893908},
}