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@ARTICLE{Longo:903441,
author = {Longo, M. and Heigl, R. J. and Schrader, Tobias Erich},
title = {{R}eal-time investigation of {L}ysozyme crystallization
kinetics: {A} neutron diffraction study},
journal = {Journal of crystal growth},
volume = {576},
issn = {0022-0248},
address = {Amsterdam [u.a.]},
publisher = {Elsevier},
reportid = {FZJ-2021-05120},
pages = {126362},
year = {2021},
abstract = {The isothermal crystallization kinetics of hen-egg-white
Lysozyme has been investigatedby means of a time-resolved
neutron diffraction experiment for almost 3 days,starting
from a supersaturated solution of Lysozyme (30 mg/ml, 3 wt
$\%$ NaCl, pD 4.75at 298 K) until the growth of crystals, in
order to have complementary informationabout the
crystallization kinetics. The temporal evolution of the
intensity of the Braggpeaks, observed in the neutron
diffraction images when a single crystal appears, hasbeen
studied. Simultaneously, the analysis of the small angle
neutron scattering curvesfrom the Lysozyme solution, during
the crystallization process, has been performed.A correlated
behaviour between the decrease of the Lysozyme concentration
and theincrease of the crystallization fraction was
observed. The crystallization kinetics wasdescribed by means
of the Johnson-Mehl-Avrami-Kolmogorov model and
parameterscompatible with our previous Lysozyme
crystallization study have been found.The Lysozyme
crystallization under constant neutron flux underlines the
known strengthof neutrons in studying biological samples
without causing radiation damage.},
cin = {JCNS-FRM-II / JCNS-4 / MLZ / JCNS-1},
ddc = {540},
cid = {I:(DE-Juel1)JCNS-FRM-II-20110218 /
I:(DE-Juel1)JCNS-4-20201012 / I:(DE-588b)4597118-3 /
I:(DE-Juel1)JCNS-1-20110106},
pnm = {6G4 - Jülich Centre for Neutron Research (JCNS) (FZJ)
(POF4-6G4) / 632 - Materials – Quantum, Complex and
Functional Materials (POF4-632)},
pid = {G:(DE-HGF)POF4-6G4 / G:(DE-HGF)POF4-632},
experiment = {EXP:(DE-MLZ)BIODIFF-20140101},
typ = {PUB:(DE-HGF)16},
UT = {WOS:000712269600001},
doi = {10.1016/j.jcrysgro.2021.126362},
url = {https://juser.fz-juelich.de/record/903441},
}