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| 001 | 906268 | ||
| 005 | 20240712112827.0 | ||
| 024 | 7 | _ | |a 10.1002/elsa.202100208 |2 doi |
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| 037 | _ | _ | |a FZJ-2022-01334 |
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| 100 | 1 | _ | |a Lu, Xin |0 P:(DE-Juel1)180280 |b 0 |u fzj |
| 245 | _ | _ | |a Tuning the moisture stability of multiphase β‐Li 3 PS 4 solid electrolyte materials |
| 260 | _ | _ | |a Weinheim |c 2022 |b Wiley-VCH Verlag GmbH & Co KGaA |
| 336 | 7 | _ | |a article |2 DRIVER |
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| 520 | _ | _ | |a Efficiently improving the moisture stability of β-Li3PS4 materials could significantly reduce production costs and eventually enable the mass application. Nanoporous multiphase β-Li3PS4 materials prepared via solvent-assistant routes usually contain solvent or solvent decomposition segments associated with the amorphous Li3PS4 phase in their structures. Herein, the solvent ethyl propionate (EP) remains in the β-Li3PS4 even after 220 h of annealing at 220°C. The possibility of tuning the moisture stability of β-Li3PS4 by adjusting the content of the solvent is investigated by environmental scanning electron microscopy (ESEM) combined with other structural analysis techniques. The results demonstrated that the hydrogen-containing amorphous Li3PS4 not only stabilizes the β-phase at room temperature but also improves the moisture stability of the material. Although the rapid hydrolysis occurs on the surface of solvent-containing β-Li3PS4 materials under ambient conditions within 10 s, with 4 wt% EP content, the material can be exposed to 1.6% relative humidity (R.H.) for at least 8 h without any structural or microstructural change. Even with the lower amount of EP (1.2 wt%) in the Li3PS4 structure, the material can withstand 1% R.H. for more than 8 h, which allows the material to be manufactured in a dry room. Our observation proposes a simple method to slightly modify the moisture stability of β-Li3PS4 to match the different manufacturing conditions. |
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| 700 | 1 | _ | |a Windmüller, Anna |0 P:(DE-Juel1)188297 |b 3 |u fzj |
| 700 | 1 | _ | |a Tsai, Chih-Long |0 P:(DE-Juel1)156244 |b 4 |u fzj |
| 700 | 1 | _ | |a Tempel, Hermann |0 P:(DE-Juel1)161208 |b 5 |u fzj |
| 700 | 1 | _ | |a Yu, Shicheng |0 P:(DE-Juel1)161141 |b 6 |e Corresponding author |
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| 773 | _ | _ | |a 10.1002/elsa.202100208 |0 PERI:(DE-600)2984616-X |n 2 |p e2100208 |t Electrochemical science advances |v 3 |y 2022 |x 2698-5977 |
| 856 | 4 | _ | |u https://juser.fz-juelich.de/record/906268/files/Electrochemical%20Science%20Adv%20-%202022%20-%20Lu%20-%20Tuning%20the%20moisture%20stability%20of%20multiphase%20%E2%80%90Li3PS4%20solid%20electrolyte%20materials.pdf |y OpenAccess |
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