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000908321 1001_ $$0P:(DE-Juel1)161336$$aBalaguer, Maria$$b0$$eCorresponding author
000908321 245__ $$aCharacterization of Y and Mn co-substituted BaZrO3 ceramics: Material properties as a function of the substituent concentration
000908321 260__ $$aAmsterdam [u.a.]$$bElsevier Science$$c2022
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000908321 520__ $$aInnovations in materials science are the key element for solving technological challenges. Various energy and environmental applications require designing materials with tailored compositions, microstructures and specific target-oriented performance. Y and Mn co-substituted BaZrO3, e.g. BaZr0.85Y0.15Mn0.05O3-δ, has previously attracted attention as a membrane material for H2 separation from gas mixtures due to its mixed proton-electron conductivity leading to appreciable levels of H2-flux at elevated temperatures and its good thermo-chemical stability under reducing environments. In the present work, we developed ceramic materials within the BaZr0.8Y0.2-xMnxO3-δ series, where x = 0.02–0.15. The study of their functional properties in dependence of the Y-to-Mn ratio disclosed that thermal expansion and hydration decrease by increasing the Mn content as well as the total electrical conductivity. In addition to that, XPS analysis and near edge X-ray absorption fine structure spectra (NEXAFS) in the vicinity of O K-edge and Mn L2,3-edges indicated that the Mn atoms oxidation state in the surface and in the bulk range from Mn2+ to Mn4+ depending on the ambient conditions that can be encountered in MPEC electrodes, which it is suggested to be related with a hydration mechanism mediated by Mn oxidation and subsequent proton attachment to oxygen neighbors, similar to LSM.
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000908321 7001_ $$0P:(DE-Juel1)159368$$aSohn, Yoo Jung$$b1$$ufzj
000908321 7001_ $$0P:(DE-Juel1)129739$$aKobertz, Dietmar$$b2
000908321 7001_ $$0P:(DE-HGF)0$$aKasatikov, Sergey$$b3
000908321 7001_ $$0P:(DE-Juel1)161352$$aFantin, Andrea$$b4
000908321 7001_ $$0P:(DE-Juel1)129765$$aMüller, Michael$$b5$$ufzj
000908321 7001_ $$0P:(DE-Juel1)129636$$aMenzler, Norbert H.$$b6$$ufzj
000908321 7001_ $$0P:(DE-Juel1)161591$$aGuillon, Olivier$$b7$$ufzj
000908321 7001_ $$0P:(DE-Juel1)129617$$aIvanova, Mariya$$b8$$eCorresponding author$$ufzj
000908321 773__ $$0PERI:(DE-600)1500750-9$$a10.1016/j.ssi.2022.115959$$gVol. 382, p. 115959 -$$p115959 -$$tSolid state ionics$$v382$$x0167-2738$$y2022
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