Journal Article FZJ-2019-04068

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Laser-Induced Desorption of co-deposited Deuterium in Beryllium Layers on Tungsten

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2019
Elsevier Amsterdam [u.a.]

Nuclear materials and energy 19, 503 - 509 () [10.1016/j.nme.2019.04.007]

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Abstract: For the development of the tritium monitoring system in ITER the hydrogen isotope release by Laser-Induced Desorption (LID) from Be layers is studied to determine the laser parameters for a high desorption efficiency while minimising dust production and surface modifications is also pursued. Be layers of 1 µm thickness with 25–30 at% D and 3 × 1022 D/m2 comparable to JET-ILW areal concentrations [1] have been produced by High Power Impulse Magnetron Sputtering (HiPIMS) on ITER grade W. Laser pulses of 1, 5 and 10 ms duration heat the layer in vacuum in the Fuel REtention DIagnostic Setup (FREDIS) and release the retained D thermally. By mass spectrometry in FREDIS and subsequent Nuclear Reaction Analysis (NRA) inside the laser spot the desorbed and remaining D is quantified. While a pulse duration of 1 ms cannot fully desorb the deuterium, it is found that a single 5 or 10 ms laser pulse with an absorbed energy density of ca. 1.5 MJ/m2 corresponding to a heat flux factor around 20 MW√s/m2 leads to nearly complete desorption of the retained D. This encourages the development of a useful tritium monitoring system, although the present layers produce some dust due to local delamination of the layer on at least 11% of the heated surface (at 1.4 MJ/m2 absorbed energy within 5 ms) and lead to unavoidable crack formation.

Classification:

Contributing Institute(s):
  1. Plasmaphysik (IEK-4)
  2. Werkstoffsynthese und Herstellungsverfahren (IEK-1)
  3. Werkstoffstruktur und -eigenschaften (IEK-2)
Research Program(s):
  1. 174 - Plasma-Wall-Interaction (POF3-174) (POF3-174)

Appears in the scientific report 2019
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Creative Commons Attribution-NonCommercial-NoDerivs CC BY-NC-ND 4.0 ; DOAJ ; OpenAccess ; Clarivate Analytics Master Journal List ; DOAJ Seal ; Emerging Sources Citation Index ; SCOPUS ; Web of Science Core Collection
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Dokumenttypen > Aufsätze > Zeitschriftenaufsätze
Institutssammlungen > IMD > IMD-2
Institutssammlungen > IMD > IMD-1
Institutssammlungen > IFN > IFN-1
Workflowsammlungen > Öffentliche Einträge
IEK > IEK-2
IEK > IEK-4
IEK > IEK-1
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Open Access

 Datensatz erzeugt am 2019-08-05, letzte Änderung am 2024-07-11


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