Journal Article FZJ-2021-01474

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3-Dimensional analysis of layer structured samples with high depth resolution using picosecond laser-induced breakdown spectroscopy

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2020
Elsevier Amsterdam

Applied surface science 532, 147185 - () [10.1016/j.apsusc.2020.147185]

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Abstract: 3-Dimensional (3D) analysis is crucial for many materials and can be used to study their structure and properties. Laser-Induced Breakdown Spectroscopy (LIBS) is a versatile tool to get depth information quickly, but the poor depth resolution and in general a difficult quantification are the two main drawbacks. To solve these problems, a LIBS method based on picosecond-laser pulses is introduced. The ablation depth is measured and associated with the laser pulse number. A series of layer-structured graphite samples was tested by this method and the 2D and 3D layer structures of these samples were identified with a resolution of up to 24 and 102 nm for Mo and C elements under a residual pressure of 1 × 10−5 Pa, respectively. This shows the great potential of picosecond Laser-Induced Breakdown Spectroscopy (ps-LIBS) in the field of depth analysis.

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Contributing Institute(s):
  1. Plasmaphysik (IEK-4)
Research Program(s):
  1. 174 - Plasma-Wall-Interaction (POF3-174) (POF3-174)

Appears in the scientific report 2021
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Medline ; Creative Commons Attribution-NonCommercial-NoDerivs CC BY-NC-ND 4.0 ; Embargoed OpenAccess ; Clarivate Analytics Master Journal List ; Current Contents - Engineering, Computing and Technology ; Current Contents - Physical, Chemical and Earth Sciences ; Ebsco Academic Search ; Essential Science Indicators ; IF >= 5 ; JCR ; NationallizenzNationallizenz ; SCOPUS ; Science Citation Index Expanded ; Web of Science Core Collection
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 Record created 2021-03-24, last modified 2024-07-08


Published on 2020-07-16. Available in OpenAccess from 2022-07-16.:
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