Journal Article FZJ-2021-03968

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Magnetic investigations on irradiation-induced nanoscale precipitation in reactor pressure vessel steels: A first-order reversal curve study

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2021
Elsevier Science Amsterdam [u.a.]

Journal of nuclear materials 552, 152973 () [10.1016/j.jnucmat.2021.152973]

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Abstract: We have investigated magnetic properties for reactor pressure vessel model alloys with variable Cu con- tents, subjected to neutron irradiation up to a fluence of 9 × 10 19 n cm −2 . Unlike a monotonic increase of microhardness with neutron fluence, the major-loop coercivity decreases at a higher fluence and the decrease becomes larger for the alloy containing a higher amount of Cu. The measurements of first-order reversal curves (FORCs) for the high-Cu alloy show that the position of the FORC distribution peak shifts toward a lower coercivity just after neutron irradiation, followed by a slight increase, associated with the broadening along both the coercivity and interaction field axes. The results can be explained by the enhancement of magnetic inhomogeneity in a matrix due to Cu precipitation and an increasing magne- tostatic interaction between local magnetic regions with different coercivity. The magnetic method using FORCs can be a possible technique which provides in-depth information on microstructural changes due to neutron irradiation, which is not obtained by measurements of a conventional major hysteresis loop.

Keyword(s): Engineering, Industrial Materials and Processing (1st) ; Materials Science (2nd)

Classification:

Contributing Institute(s):
  1. JCNS-FRM-II (JCNS-FRM-II)
  2. Streumethoden (JCNS-2)
  3. JCNS-4 (JCNS-4)
  4. Heinz Maier-Leibnitz Zentrum (MLZ)
Research Program(s):
  1. 6G4 - Jülich Centre for Neutron Research (JCNS) (FZJ) (POF4-6G4) (POF4-6G4)
  2. 632 - Materials – Quantum, Complex and Functional Materials (POF4-632) (POF4-632)
Experiment(s):
  1. KWS-1: Small angle scattering diffractometer (NL3b)

Appears in the scientific report 2021
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Medline ; Creative Commons Attribution-NonCommercial-NoDerivs CC BY-NC-ND 4.0 ; Embargoed OpenAccess ; Clarivate Analytics Master Journal List ; Current Contents - Engineering, Computing and Technology ; Current Contents - Physical, Chemical and Earth Sciences ; Ebsco Academic Search ; Essential Science Indicators ; IF < 5 ; JCR ; NationallizenzNationallizenz ; SCOPUS ; Science Citation Index Expanded ; Web of Science Core Collection
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Document types > Articles > Journal Article
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Institute Collections > JCNS > JCNS-2
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 Record created 2021-10-22, last modified 2021-11-30


Published on 2021-04-02. Available in OpenAccess from 2023-04-02.:
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