Journal Article FZJ-2021-03988

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Mechanical properties of cold sintered ZnO investigated by nanoindentation and micro-pillar testing

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2021
Elsevier Science Amsterdam [u.a.]

Journal of the European Ceramic Society 42(2), 512-524 () [10.1016/j.jeurceramsoc.2021.10.011]

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Abstract: Characteristic densification in cold sintered microstructures could also have a strong influence in defining their mechanical response. For the first time, nanoindentation and micro-pillar testing is used to study these details. Based on our recent work, we selected cold sintered (250 °C, ∼ 99 % dense) and conventionally sintered (900 °C, ∼ 98 % dense) ZnO samples. Hardness, elastic modulus and compressive stress of cold sintered samples were measured to be 5.5 GPa ± 0.5, 100 GPa ± 5 and ∼ 1.2 GPa, respectively. Same values for conventionally sintered ZnO were 4.8 GPa ± 0.6, 109 GPa ± 6 and 0.8 GPa, respectively. The distinctive nature of grain boundary regions in cold sintered samples were found to influence the deformation behavior of these samples, as confirmed by TEM investigations. Our study reveals the potential of cold sintering and use of selected testing techniques as suitable choice.

Keyword(s): Materials Science (2nd)

Classification:

Contributing Institute(s):
  1. Werkstoffsynthese und Herstellungsverfahren (IEK-1)
Research Program(s):
  1. 899 - ohne Topic (POF4-899) (POF4-899)
  2. SPP 1959:  Manipulation of matter controlled by electric and magnetic fields: Towards novel synthesis and processing routes of inorganic materials (274005202) (274005202)
  3. DFG project 319339707 - Diffusionsgesteuerte Prozesse in polykristallinem Ceroxid: Kombinierte Wirkung von elektrischem Feld und mechanischer Belastung (319339707)

Appears in the scientific report 2021
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Medline ; Creative Commons Attribution-NonCommercial-NoDerivs CC BY-NC-ND 4.0 ; Embargoed OpenAccess ; Clarivate Analytics Master Journal List ; Current Contents - Engineering, Computing and Technology ; Current Contents - Physical, Chemical and Earth Sciences ; Ebsco Academic Search ; Essential Science Indicators ; IF < 5 ; JCR ; SCOPUS ; Science Citation Index Expanded ; Web of Science Core Collection
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 Record created 2021-10-25, last modified 2024-07-08


Published on 2021-10-13. Available in OpenAccess from 2023-10-13.:
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