| Hauptseite > Publikationsdatenbank > Columnar grain boundaries are the weakest link in hard coatings: insights from micro-cantilever testing |
| Journal Article | FZJ-2025-04117 |
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2025
Taylor & Francis
London [u.a.]
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Please use a persistent id in citations: doi:10.1080/21663831.2025.2560526 doi:10.34734/FZJ-2025-04117
Abstract: The effect of columnar grain boundaries (GBs) on the fracture toughness was investigated using micro-cantilever fracture testing in a hard coating featuring two distinct microstructures within a single sample: a columnar-grained top and an epitaxial bottom region. Bridge-notch fracture initiated more readily in the columnar-grained region, indicating reduced toughness. Furthermore, quantitative analysis of the load drops at bridge-failure confirmed a ∼30% decrease in fracture toughness due to GBs: from 4.1 to 3.0 MPa m1/2. These results reveal the detrimental role of GBs in fracture toughness and highlight the importance of microstructural design for improving the mechanical performance of hard coatings.
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