Journal Article FZJ-2018-05152

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Enhancing efficiency of field assisted sintering by advanced thermal insulation

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2018
Elsevier Amsterdam [u.a.]

Journal of materials processing technology 262, 326 - 339 () [10.1016/j.jmatprotec.2018.07.008]

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Abstract: The influence of advanced thermal insulation on energy consumption and temperature distribution during electric field assisted sintering of conductive stainless steel powder and non-conductive zirconia powder was investigated. Four types of tool setup were considered: i) without insulation, ii) with die wall insulation, iii) with additional insulation of die faces and iv) with spacers manufactured from carbon fiber reinforced carbon composite (CFRC). The influence of thermal insulation on energy consumption was experimentally studied for samples with diameter of 17 mm. The temperature distribution in samples with diameters of 17 mm, 50 mm and 150 mm was modeled using the Finite Element Method. The power consumed during dwell was almost half the value when die wall insulation was used. The additional insulation of die faces and the application of CFRC spacers provide a threefold decrease in power during sintering of steel powder and a fivefold reduction during sintering of zirconia powder. The advanced thermal insulation significantly homogenizes the temperature distribution within samples of small and medium size. The advanced thermal insulation provides a strong decrease in the temperature gradient inside large conductive sample with a diameter of 150 mm. However, insulation apparently cannot ensure acceptable temperature homogeneity within non-conductive parts of such diameter. The reason for this is the specific current path and related heat concentration near the sample edge.

Classification:

Contributing Institute(s):
  1. Werkstoffsynthese und Herstellungsverfahren (IEK-1)
Research Program(s):
  1. 899 - ohne Topic (POF3-899) (POF3-899)

Appears in the scientific report 2018
Database coverage:
Embargoed OpenAccess ; Current Contents - Engineering, Computing and Technology ; Ebsco Academic Search ; IF < 5 ; JCR ; SCOPUS ; Science Citation Index Expanded ; Thomson Reuters Master Journal List ; Web of Science Core Collection
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 Record created 2018-08-29, last modified 2024-07-08


Published on 2018-07-07. Available in OpenAccess from 2020-07-07.:
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