Hauptseite > Publikationsdatenbank > Hydrothermal synthesis, off-axis electron holography and magnetic properties of Fe$_{3}$O$_{4}$ nanoparticles |
Contribution to a conference proceedings/Journal Article | FZJ-2015-02907 |
; ; ; ;
2014
IOP Publ.
Bristol
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Please use a persistent id in citations: http://hdl.handle.net/2128/8552 doi:10.1088/1742-6596/522/1/012062
Abstract: The hydrothermal synthesis of Fe3O4 nanoparticles (NPs) (< 50 nm) from mixed FeCl3 / FeCl2 precursor solution at pH ~ 12 has been confirmed using complementary characterisation techniques of transmission electron microscopy and X-ray diffractometry. Off-axis electron holography allowed for visualisation of their single domain (SD) nature, as well as inter-particle interactions, with the latter attributed to explain the pseudo-SD/multi-domain behaviour demonstrated by bulk magnetic measurements.
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