Journal Article FZJ-2024-06168

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Enabling quantitative analysis of in situ TEM experiments: A high-throughput, deep learning-based approach tailored to the dynamics of dislocations

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2025
Elsevier Science Amsterdam [u.a.]

Acta materialia 282, 120455 - () [10.1016/j.actamat.2024.120455]

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Abstract: In situ TEM is by far the most commonly used microscopy method for imaging dislocations, i.e., line-like defects in crystalline materials. However, quantitative image analysis so far was not possible, implying that also statistical analyses were strongly limited. In this work, we created a deep learning-based digital twin of an in situ TEM straining experiment, additionally allowing to perform matching simulations. As application we extract spatio-temporal information of moving dislocations from experiments carried out on a Cantor high entropy alloy and investigate the universality class of plastic strain avalanches. We can directly observe “stick–slip motion” of single dislocations and compute the corresponding avalanche statistics. The distributions turn out to be scale-free, and the exponent of the power law distribution exhibits independence on the driving stress. The introduced methodology is entirely generic and has the potential to turn meso-scale TEM microscopy into a truly quantitative and reproducible approach.

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Contributing Institute(s):
  1. Materials Data Science and Informatics (IAS-9)
Research Program(s):
  1. 5111 - Domain-Specific Simulation & Data Life Cycle Labs (SDLs) and Research Groups (POF4-511) (POF4-511)

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Medline ; Creative Commons Attribution-NonCommercial-NoDerivs CC BY-NC-ND 4.0 ; OpenAccess ; Clarivate Analytics Master Journal List ; Current Contents - Engineering, Computing and Technology ; Current Contents - Physical, Chemical and Earth Sciences ; Ebsco Academic Search ; Essential Science Indicators ; IF >= 5 ; JCR ; SCOPUS ; Science Citation Index Expanded ; Web of Science Core Collection
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 Record created 2024-11-11, last modified 2025-02-03


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