Home > Publications database > Convenient Preparation of High-Quality Specimens for Annealing Experiments in the Transmission Electron Microscope |
Journal Article | FZJ-2015-00877 |
; ;
2014
Cambridge University Press
New York, NY
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Please use a persistent id in citations: doi:10.1017/S1431927614013476
Abstract: A procedure based on focused ion beam milling and in situ lift-out is introduced for the preparation of high-quality specimens for in situ annealing experiments in the transmission electron microscope. The procedure allows an electron-transparent lamella to be cleaned directly on a heating chip using a low ion energy and back-side milling in order to minimize redeposition and damage. The approach is illustrated through the preparation of an Al–Mn–Fe complex metallic alloy specimen.
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